Table 2-1S: Standard Methods 3030K Standard Method
Standard Methods 3030K (A24)
Microwave Assisted Digestion
Type |
Matrix |
Analytes |
Detection |
Control |
Microwave Acid Leach |
Water |
Ag, Al, As, Au, Ba, Be, Bi, Ca, Cd, Ce, Co, Cr, Cu, Hg, Ir, K, Li, Mg, Mn, Mo, Na, Ni, Os, Pb, Pd, Pt, Rh, Sb, Se, Si, Sn, Sr, Th, Ti, Tl, V, Zn |
FAAS ET-AAS CV-FAAS |
Temperature Feedback Control |
Condensed Procedure |
45 mL sample & 5 mL HNO3 Performance Criteria: Heat to 160 ± 4°C in 10 min. Slow rise to 165 - 170 ± 4°C in additional 10 min Prescription Settings: For five 120 mL PFA vessels 545 W for 10 min, 344 W for 10 min. Reaction Conditions are identical to EPA Method 3015 |