Table 2-1H: ASTM Method D5258-92 Standard Method

ASTM Method D5258-92 (A8)

Standard Practice for Acid Extraction of Elements from Sediments Using Closed Vessel Microwave Heating

Type

Matrix

Analytes

Detection

Control

Microwave

Acid Leach

Sediment

Soil

As, Cd, Cu, Mg,

Mn, Ni, Pb, Zn

Not Specified

Pressure

Feedback

Control

Condensed Procedure

1g sample and 20 mL 1:1 HNO3

Heat to 100 psi and maintain for 30 min.

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