Appendix 2. Geological and Metallurgical
Reference Materials
| Appendix 2.2 Steels and alloys | ||||||
|---|---|---|---|---|---|---|
| Matrix | Analytes | Reagents | Cavity/Vessel | MW conditions | Detection | Ref. |
BAM High-alloy steel 228-1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BAM High-alloy steel 277-1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BAM High-alloy steel 278-1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BAM High-alloy steel 328-1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BAM Ferro-chromium 530-1 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BAM Ferro-chromium 533-1 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BAM High-alloy steel CrMnMoNiTi1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BAM High-alloy steel CrNiSiMn1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS Ferro-chromium 203/2 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BCS Ferro-chromium 204/1 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BCS Ferro-manganese 208/1 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4, HNO3 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BCS High-alloy steel 211/1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS Ferro-manganese 280 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4, HNO3 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
BCS Fe-Si alloy 305 |
Al, Ca, Cr, Cu, Fe, Hf, Mn, Ni, Ru, Si, Ti, Zr | H3PO4 | Multimode/ open |
10-15 min to 150-200°C | ICP-OES | F30 |
BCS High-alloy steel 338 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS High-alloy steel 339 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS High-alloy steel 340 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS High-alloy steel 341 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS High-alloy steel 342 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BCS Nickel alloy 345 |
As | HNO3, HF | Multimode/ LP closed |
15 min at 200 W, 15 min at 325 W, 30 min at 260 W |
HG-AAS | F31 |
BCS Nickel alloy 346 |
As | HNO3, HF | Multimode/ LP closed |
15 min at 200 W, 15 min at 325 W, 30 min at 260 W |
HG-AAS | F31 |
| As | HNO3, HF | Multimode/ LP closed |
15 min at 200 W, 15 min at 325 W, 30 min at 260 W |
HG-AAS | F32 | |
BCS Steel 452 |
As, Cr, Cu, Mn, Ni, P, Si, Sn, Ti, W | HNO3, HCl, HF | Multimode/ LP closed |
80 sec at 625 W | DCP-OES | F33 |
BCS High-alloy steel JK 8F |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
BRAMMER Slag ST-100 |
Ca, Fe, Mg, Mn, Si | HCl, HF, HNO3 | Multimode/ LP closed |
2 min at 650 W | F-AAS | F14 |
CSAN Ferro silicon 4-1-01 |
Al, Ca, Cr, Cu, Fe, Hf, Mn, Ni, Ru, Si, Ti, Zr | H3PO4 | Multimode/ open |
10-15 min at 150-200°C | ICP-OES | A30 |
CSAN Ferro silicon 4-1-02 |
Al, Ca, Cr, Cu, Fe, Hf, Mn, Ni, Ru, Si, Ti, Zr | H3PO4 | Multimode/ open |
10-15 min at 150-200°C | ICP-OES | F30 |
CSAN Ferro chromium 4-2-01 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro chromium 4-2-02 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro chromium 4-2-03 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro chromium 4-2-04 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro manganese 4-3-01 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro manganese 4-3-02 |
Al, Co, Cr, Cu, Fe, Mn, Mo, Ni, Si, Ti, V | H2SO4, H2O, H3PO4 | Multimode/ LP closed |
10 min at 330 W | ICP-OES | F29 |
CSAN Ferro manganese silicon 4-5-02 |
Al, Ca, Cr, Cu, Fe, Hf, Mn, Ni, Ru, Si, Ti, Zr | H3PO4 | Multimode/ open |
10-15 min at 150 - 200°C | ICP-OES | F30 |
CSAN Ferro chromium silicon 4-5-03 |
Al, Ca, Cr, Cu, Fe, Hf, Mn, Ni, Ru, Si, Ti, Zr | H3PO4 | Multimode/ open |
10-15 min at 150 - 200°C | ICP-OES | F30 |
IFM Slag 7 |
Al, Ca, Fe, K, Mg, Mn, Na, Ti, Si | A. 1. HCl, HF 2. HBO3 B. 1. HCl, HF, H2SO4 2. HBO3 C. 1. Aqua regia, HF 2. HBO3 D. 1. HCl, HF, H2O2 2. HBO3 |
LP closed Multimode/ LP closed Multimode/ LP closed Multimode/ LP closed |
1. Same as A 1. Same as A 1. Same as A |
F-AAS | A8 |
IRSID High-alloy steel 204-1 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST High-alloy stainless steel 73 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST High-alloy stainless steel 101 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST Stainless steel Cr-Ni-Ti 121 |
- | HCl, HNO3, HF | Multimode/ LP closed |
30 sec at 300 W (x2) | - | F17 |
NIST Solder 40 Sn - 60 Pb 127 |
- | HBF4, H2O, HNO3 | Multimode/ LP closed |
Varying time at 600 W | - | F17 |
NIST High alloy stainless steel 133 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST High alloy stainless steel 160 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST High alloy steel 161 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST Nickel copper alloy 162 |
Al, Cu, Fe, Mn, Ni, Si | HCl, HF, HNO3 | Multimode/ LP closed |
2 min at 650 W | F-AAS | F14 |
NIST High alloy steel 168 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
| - | HF, HNO3, H2O | Multimode/ LP closed |
5 min at 600 W | - | F17 | |
NIST LA steel high silicon 179 |
Al, Cr, Cu, Mn, Mo, Ni, P, Si, Sn, Ti, V | HNO3, HCl, HF | Multimode/ LP closed |
80 sec at 625 W | DCP-OES | F33 |
NIST High-alloy stainless steel 343 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST High-alloy valve steel 346 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST Waspalloy Ni-Co-Cr 349 |
Co, Cr, Fe, Mo, Ni, W | HCl, HF, HNO3 | Multimode/ LP closed |
30 sec at 325 W | ICP-OES | F34 |
NIST Cast iron steel 890 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
NIST Cast iron steel 892 |
Cr | 1. HNO3, HCl, HF 2. HNO3 |
Multimode/ LP closed |
1. 15 min at 55% 2. 15 min at 55% (if incompletely digested) |
Titration with Fe(II) | F28 |
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